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Synthesis of Secondary and Tertiary Alkylboranes via Formal Hydroboration of Terminal and 1,1-Disubstituted Alkenes
... 1,1-disubstituted alkenes with bis(pinacolato)diboron and methanol provides products with ... favoring the branched isomer. Subsequent photocatalytic cross-couplings using iridium and nickel cocatalysis enable a ...
... 3-position using an iridium catalyst and boron pinacolate (67% over two steps) ... Coupling of the two halves was no problem- including the final deprotection, the ...