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Synthesis of isothiocyanates

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A novel and highly selective method uses triphenylphosphine, diethylazodicarboxylate and NH4SCN for the conversion of alcohols, thiols, carboxylic acids, silyl ethers, and silyl carboxylates to their corresponding thiocyanates.
N. Iranpoor, H. Firouzabadi, B. Akhlaghinia, R. Azadi, Synthesis, 2004, 92-96.