Polystyrene-Supported Benzenesulfonyl Azide: A Diazo Transfer Reagent That Is Both Efficient and Safe
Gary M. Green, Norton P. Peet and William A. Metz
Aventis Pharmaceuticals, Route 202-206, Bridgewater, New Jersey 08807, USA
G. M. Green, N. P. Peet, W. A. Metz, J. Org. Chem., 2001, 66, 2509-2511.
DOI: 10.1021/jo005738d
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Abstract
Sulfonyl azides are potentially hazardous due to their propensity for explosive decomposition under various reaction conditions. Polymer-supported benzenesulfonyl azide provides a diazo transfer reagent with improved process safety characteristics and thus offers an excellent reactant for laboratory use.
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Key Words
α-Diazo Esters, α-Diazo Ketones
ID: J42-Y2001
