Waste-Free and Environment-Friendly Uncatalyzed Synthesis of Dithiocarbamates under Solvent-Free Conditions
Najmedin Azizi, Forogh Ebrahimi, Elham Aakbari, Fezzeh Aryanasab, Mohammad R. Saidi*
*Department of Chemistry, Sharif University of Technology, P. O. Box 11465-9516, Tehran 11365, Email: saidisharif.edu
N. Azizi, F. Ebrahimi, E. Aakbari, F. Aryanasab, M. R. Saidi, Synlett, 2007, 2797-2800.
A mild, convenient, and practical one-pot procedure gives dithiocarbamates in good to excellent yields by condensation of amines, CS2, and a Michael acceptor, under solvent-free conditions at room temperature.
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N. Azizi, F. Aryanasab, M. R. Saidi, Org. Lett., 2006, 8, 5275-5277.