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Efficient Microwave-Assisted Synthesis of N-(tert-Butylsulfinyl)imines Catalyzed by Amberlist-15

Chakrapani Sanaboina, Samaresh Jana*, Laxminarayana Eppakayala

*Department of Chemistry, School of Applied Sciences, KIIT University, Bhubaneswar-751024, Odisha, India, Email: sjanafchkiit.ac.in

C. Sanaboina, S. Jana, L. Eppakayala, Synlett, 2014, 25, 1006-1008.

DOI: 10.1055/s-0033-1340858 (free Supporting Information)


Abstract

Use of the heterogeneous catalyst amberlist-15 A enables an efficient synthesis of N-(tert-butylsulfinyl)imines under microwave irradiation. Amberlist-15 is convenient to handle, inexpensive, safe to use and quickly separable from the reaction mixture. This method offers a number of advantages including operational simplicity, high yield of products, and broad substrate scope.


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Key Words

N-sulfinyl imines, building blocks, microwave synthesis, heterogeneous catalyst, aldehydes


ID: J60-Y2014