Categories: C-N Bond Formation >
Synthesis of imides
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Protecting Groups
Recent Literature
A manganese pincer complex catalyzes a dehydrogenative coupling of diols and
amines to form cyclic imides. The reaction forms hydrogen gas as the sole
byproduct, making the overall process atom economical and environmentally benign.
N. Angel Espinosa-Jalapa, A. Kumar, G. Leitus, Y. Diskin-Posner, D. Milstein, J. Am. Chem. Soc., 2017,
139, 11722-11725.
An economical and practical method for the synthesis of a wide range of imide
derivatives has been developed by using inexpensive and readily available
reagents under mild conditions.
P. Y. Reddy, S. Kondo, T. Toru, Y. Ueno, J. Org. Chem., 1997,
62, 2652-2654.
A Lewis acid catalyzed and solvent free procedure for the preparation of imides
from the corresponding anhydrides uses TaCl5-silica gel as Lewis acid
under microwave irradiation.
S. Chandrasekhar, M. Takhi, G. Uma, Tetrahedron Lett., 1997,
38, 8089-8092.