Categories: C-O Bond Formation >
Synthesis of Nitrites
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Recent Literature
Alkyl nitrites were prepared in good to excellent yields by treatment of
alcohols and thiols with
triphenylphosphine/2,3-dichloro-5,6-dicyanobenzoquinone/Bu4NNO2 in acetonitrile.
This method allows a selective conversion of primary alcohols in the presence of secondary and tertiary alcohols and thiols.
B. Akhlaghinia, A. R. Pourali, Synthesis,
2004,
1747-1749.
