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Categories: C-O Bond Formation

Synthesis of O,S-Acetals


Recent Literature

A highly selective, environmentally friendly, and scalable electrochemical α-C(sp3)-H acyloxylation of sulfides enables the construction of α-acyloxy sulfides. The method offers exceptionally broad substrate scope, high regioselectivity, gram-scale synthesis, and construction of complex molecules.
H. Wang, M. He, Y. Li, H. Zhang, D. Yang, M. Nagasaka, Z. Lv, Z. Guan, Y. Cao, F. Gong, Z. Zhou, J. Zhu, S. Samanta, A. D. Chowdhury, A. Lei, J. Am. Chem. Soc., 2021, 143, 3628-3637.